Winter 2002 CHEMISTRY 30AL LABORATORY SCHEDULE AND ASSIGNMENTS SAFETY GLASSES AND LAB COATS MUST BE WORN INTHE LABORATORY AT ALL TIMES. FAILURE TO DO SO WILL RESULT IN DISMISSAL FROM THE LABORATORY. Week Date Experiment1 Reading 2 Videotape3 Lecture Text4,5 Due Date 6_ 1 1/8, 1/9 10 – Synthesis of Aspirin 6-27 Safety (#5805) 643 (BF) 1 1/10, 1/11 Analysis of Aspirin (part 1) 109-119 Recrystallization (#3135) 1/17, 1/18 2 1/15, 1/16 11 – Synthesis of an Iron Oxalate Complex 32-38 Melting Point 2 1/17, 1/18 Analysis of an Iron Oxalate Complex(1) Determination (#3138) 685-700 (M) 3 1/22, 1/23 Analysis of an Iron Oxalate Complex(2) 1/29, 1/30 3 1/24, 1/25 13 – Extraction of Caffeine 123–138; 380-384 Extraction (#3132) 550-555 (M) 4 1/29, 1/30 MS, UV, IR Analysis of Caffeine 283-303 Intro to MS Tutorial (SLC) 499-520; 910-917(BF) 2/7, 2/8 4 1/31, 2/1 14 – IR; Chemical Structure 242-282 IR (#3139) 427-445 (BF) 2/7, 2/8 5 2/5, 2/6 8 – Simple Distillation 142-148 Simple Distillation (#3141) 420-428 (M) 5 2/7, 2/8 8 – Gas Chromatography 62-67 Gas Chromatography (#3134) 2/14, 2/15 6 2/12, 2/13 16 – Isolation and Characterization of C60 68-69,76-79 The Discovery of C60 24 (BF) 333-334 (M) 2/19, 2/20 6 2/14, 2/15 18 – 14C NMR 200-205 453-462; 475-480 (BF) 2/21, 2/22 7 2/19, 2/20 Library Assignment 747– 750 (M) 2/26, 2/27 7 2/21, 2/22 15 – Ion Exchange Chromatography 68-81 Column Chromatography (#2311) 8 2/26, 2/27 Ion Exchange Chromatography 3/5, 3/6, 8 2/28, 3/1 19 – Group Project: Soil Analysis 127-129 25-26, 772-777 (BF) 9 3/5, 3/6 Soil Analysis (continued) 9 3/7, 3/8 Soil Analysis (continued) 1 Chemistry Experiements for Physical Science and Engineering Majors A.A. Russell and M.M. Henary, Burgess Publishing 1999 2 Organic Chemistry, 4th Ed. J. A. Landgrebe, Brooks/Cole Publishing Co. 1993 (L) 3 Instructional Media Library, Powell 270 or online at http://www.oid.ucla.edu/webcast/chemistry 4 Organic Chemistry 3rd Ed. W.H. Brown and C.S. Foote; Saunders College Publishing 2001 (BF) 5 Principles of Chemistry Munowitz, W. W. Norton and Company, Inc. 2000 (M) 6 Pre-lab reports and assignments are due at the beginning of the lab period; observations and data are due at the end of the lab period in which the data are collected; post-lab reports are due at the beginning of your regularly scheduled lab period on the listed due date. Each student is responsible for their own report for due dates that are in bold face. All other post-lab reports will be submitted by a group, with the individual effort of each lab member noted in the report.10 3/12, 3/13 Soil Analysis (continued) 3/14, 3/15 10 3/14, 3/15 Oral Reports on Group ProjectsDue Dates for Assignment Reports, CPR Writing Assignments, and Exams Week Category Topic Due Dates Report Quiz/Exam CPR 1 2 10 Synthesis and Analysis of Aspirin Jan 17, 18 2 1 Assignment 10; Lectures 1 and 2 Jan 17, 18 3 4 11 Synthesis and Analysis of an Iron Oxalate Compound Jan 29, 30 4 2 Assignment 11, Lecture 3 Jan 31, Feb 1 5 1 3-D Angles Essay: Feb 4 – 8 Reviews: Feb 9 - 12 5 13 Extraction of Caffeine Feb 7, 8 5 14 IR Feb, 7, 8 6 8 Simple Distillation and Gas Chromatography Feb 14, 15 6 3 Assignments 13, 14, and 8; Lectures 4 and 5 Feb 14, 15 6 2 The Discovery of C60 Essay:: Feb 14 – 19 Reviews: Feb 20 -24 7 16 Isolation and Characterization of C60 Feb 19, 20 7 1814C NMR Feb 21, 22 8 X Library Assignment Feb 26, 27 8 4 Assignments 16, 18 and X; Lecture 6 Feb 28, Mar 1 8 3 Identify a Compound Essay:: Feb 28 – Mar 5 Reviews: Mar 6 - 11 9 15 Ion Exchange Chromatography Mar 5, 6 10 19 Oral Presentations Mar 14, 15 Finals Week Cumulative Exam with emphasis on Lectures 7, and 8; Assignments 15, and 19 Tuesday
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