Winter 2002 CHEMISTRY 30AL LABORATORY SCHEDULE AND ASSIGNMENTS SAFETY GLASSES AND LAB COATS MUST BE WORN INTHE LABORATORY AT ALL TIMES FAILURE TO DO SO WILL RESULT IN DISMISSAL FROM THE LABORATORY Week Date Experiment1 Reading 2 Videotape3 1 1 1 8 1 9 1 10 1 11 10 Synthesis of Aspirin Analysis of Aspirin part 1 2 2 1 15 1 16 1 17 1 18 11 Synthesis of an Iron Oxalate Complex Analysis of an Iron Oxalate Complex 1 3 3 1 22 1 23 1 24 1 25 Analysis of an Iron Oxalate Complex 2 13 Extraction of Caffeine 123 138 380 384 Extraction 3132 550 555 M 4 4 1 29 1 30 1 31 2 1 MS UV IR Analysis of Caffeine 14 IR Chemical Structure 283 303 242 282 Intro to MS Tutorial SLC IR 3139 499 520 910 917 BF 427 445 BF 5 5 2 5 2 6 2 7 2 8 8 Simple Distillation 8 Gas Chromatography 142 148 62 67 Simple Distillation 3141 Gas Chromatography 3134 420 428 M 6 6 2 12 2 13 2 14 2 15 16 Isolation and Characterization of C60 18 14C NMR The Discovery of C60 24 BF 333 334 M 453 462 475 480 BF 7 7 2 19 2 20 2 21 2 22 Library Assignment 15 Ion Exchange Chromatography 68 81 8 8 2 26 2 27 2 28 3 1 Ion Exchange Chromatography 19 Group Project Soil Analysis 127 129 9 9 3 5 3 6 3 7 3 8 1 2 3 4 5 6 6 27 109 119 Safety 5805 Recrystallization 3135 32 38 Melting Point Determination 3138 Lecture Text4 5 68 69 76 79 200 205 Due Date 6 643 BF 1 17 1 18 685 700 M 1 29 1 30 2 7 2 8 2 7 2 8 2 14 2 15 747 750 M Column Chromatography 2311 2 19 2 20 2 21 2 22 2 26 2 27 3 5 3 6 25 26 772 777 BF Soil Analysis continued Soil Analysis continued Chemistry Experiements for Physical Science and Engineering Majors A A Russell and M M Henary Burgess Publishing 1999 Organic Chemistry 4th Ed J A Landgrebe Brooks Cole Publishing Co 1993 L Instructional Media Library Powell 270 or online at http www oid ucla edu webcast chemistry Organic Chemistry 3rd Ed W H Brown and C S Foote Saunders College Publishing 2001 BF Principles of Chemistry Munowitz W W Norton and Company Inc 2000 M Pre lab reports and assignments are due at the beginning of the lab period observations and data are due at the end of the lab period in which the data are collected post lab reports are due at the beginning of your regularly scheduled lab period on the listed due date Each student is responsible for their own report for due dates that are in bold face All other post lab reports will be submitted by a group with the individual effort of each lab member noted in the report 10 10 3 12 3 13 3 14 3 15 Soil Analysis continued Oral Reports on Group Projects 3 14 3 15 Due Dates for Assignment Reports CPR Writing Assignments and Exams Week 1 2 2 3 4 Category Report Quiz Exam Topic CPR 10 Synthesis and Analysis of Aspirin Assignment 10 Lectures 1 and 2 Jan 17 18 Jan 17 18 Jan 29 30 1 Synthesis and Analysis of an Iron Oxalate Compound Assignment 11 Lecture 3 3 D Angles 2 Extraction of Caffeine IR Simple Distillation and Gas Chromatography Assignments 13 14 and 8 Lectures 4 and 5 The Discovery of C60 1 11 4 5 2 5 5 6 6 6 13 14 8 7 7 8 8 8 16 18 X 9 10 Finals Week 15 19 Due Dates 3 Isolation and Characterization of C60 C NMR Library Assignment Assignments 16 18 and X Lecture 6 Identify a Compound 14 4 3 Ion Exchange Chromatography Oral Presentations Cumulative Exam with emphasis on Lectures 7 and 8 Assignments 15 and 19 Jan 31 Feb 1 Essay Feb 4 8 Reviews Feb 9 12 Feb 7 8 Feb 7 8 Feb 14 15 Feb 14 15 Essay Feb 14 19 Reviews Feb 20 24 Feb 19 20 Feb 21 22 Feb 26 27 Feb 28 Mar 1 Essay Feb 28 Mar 5 Reviews Mar 6 11 Mar 5 6 Mar 14 15 Tuesday March
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