Instrumental Analysis of Process Products ChE 5503 - Section 001 – Fall 2005T, TH 12:55 -01:45 PM PM Room: EMCB 122T, TH 2-5:00 PM Room: 3215 MEB Lab phone 585-5785Instructors: Terry Ring2290 MEB, 585-5705, [email protected] Hours: T 9-10:00 or by appointmentKeith Roper (Special Lectures)2284 MEB, 585-9185, [email protected] Managers: Bob Cox, Dana OverackerTextbook: The Essential Guide to Analytical Chemistry. Georg Schwedt. John Wiley & Sons, Chichester 1997.Prerequisite: CHEM 3070 and major statusDescription: Sampling, identification, and analysis of process-related materials using quantitative instrumental andlaboratory techniques. Historical and current methods. Emphasis on adaptability to on-line processmonitoring. Method development, data analysis, and standard laboratory practices are included.Spectroscopic, chromatographic and other instrumental techniques for identification and analysis ofprocess related materials.Course Goal: This course is intended to help process engineers understand the principles and limitations ofanalytical equipment commonly available in an industrial quality-control or analytical lab. Animportant part of the course will be a consideration of standard analytical methods, quantitativetechniques, and analytical alternatives. Learning Objectives: 1) Evaluate the precision and accuracy of numerical values read from or displayed by commonlaboratory apparatus (pipettes, balances, etc.)2) Design and implement valid methods for sampling, preparation and treatment of materialsintended for QA, QC or process control analysis.3) Apply common physical properties of solids and liquids in the laboratory.4) Analyze experimental data based on observations and computation of descriptive statistics.5) Apply thermal analysis concepts to TGA thermo grams.6) Apply spectroscopy concepts to typical quantitative process analytical problems utilizing UV, Vis,IR and AA instruments.7) Apply Chromatography concepts to typical quantitative process analytical problems utilizing GCand HPLC instruments.8) Design and conduct experiments to collect data relevant to analysis objectives.9) Produce professional quality memo reports on analytical activities suitable for industry.10) Perform a literature search and criticize analytical methods.11) Troubleshoot procedures and instrumental hardware problems in a time constrained laboratoryenvironment.CLEAR: Consultants for Writing, Teams and Oral Presentations are available for consultations.Oral communication and teamwork : Katie Sullivan. [email protected], MEB 2233, 581-8715.Written communication :Kelly Harward. [email protected], MEB 2233, 581-8715.Grading: Scaled curve with the highest score received corresponding to 100%Notebooks – 10%Midterms – 30%Memo Reports – 60%Add/Drop Policy: Add-Drop.pdfNotebooks: A professional laboratory note book will be required. The bookstore carries one with perforated pages and carbonless paper in it that is very useful. You can either photocopy your lab note book or tear out the carbon copy pages for handing in at the appropriate times. You need to keep your laboratory notebook current at all times so that your instructor can examine it when he/she feels like it.Exams: There will be two 50-minute closed-book midterm exams during the course of the ½ semester on thelecture materials and laboratory work. Date Lecture Topic Lab Topic Reading Lab SOP’s Material DueTH Aug25Course Overview,Guidelines forPreparation of LabReportsMEB 3215 OrientationLecturesLaboratory Safety,Making PhysicalMeasurements,Error Analysis I(TR) Ch. 1Ch. 4Physical PropertiesLabMeasuring Wt%MoistureDensity by DensityMeterReading aHydrometerRefractive Index of aLiquidQuestionnaireT Aug 30Sampling, Sample Prep.,Property Characterization(KR)Notebooks, Sampling,Measurement Techniques(practice)pp. 2-17,38-43Physical PropertiesLabBring dry dog orcat food sampleTh Sep 1Literature ReviewThermal Analysis(TR)PhysicalProperties/ThermalAnalysisCh. 6.1,6.2Thermal AnalysisPhysical PropertiesLabT Sep 6Laboratory ReportPreparation (TR),Atomic Spectroscopy(KR)PhysicalProperties/ThermalAnalysisCh. 7.1,11.6Thermal AnalysisPhysical PropertiesLabNotebooksTH Sep 8 Midterm IPhysical Properties /Atomic AbsorptionSieve Analysis Analysis for MetalsBring Gatoraid likejuice drink of youchoosingT Sep 13Intro to MolecularSpectrometry (TR)Physical Properties /Atomic AbsorptionCh. 8.1,8.2Metals in a JuiceDrinkPhysical PropertiesMemo ReportTH Sep15UV/Vis Spectrometry andColorimetry (KR)UV/Vis Introduction &Prepare StandardsCh. 8.3,8.4Prepare StandardsUV/Vis Spectra &Analysis LabTGA Memo ReportT Sep 20Infra red Spectrometry(TR)IR/FTIR Analysis Ch. 8.5IR/FTIR Spectra &Analysis LabNotebooksTH Sep22Separations andChromatography (KR)IR Analysis ProblemCh. 9.1,9.2Analysis for MetalsMemo ReportT Sep 27LC/GC Instruments andMethods (KR)Introduction to Gas &Liquid ChromatographyCh. 9.2Gas & LiquidChromatographyTH Sep29Quantitative GC,Troubleshotting (KR)Gas/Liquid AnalysisProblemCh. 9.2HPLC Procedure forTesting SugarsUV&FTIR MemoReportsT Oct 4 Midterm IIGas/Liquid AnalysisProblemTH Oct 6Process AnalyticalChemistry (TR)Open Lab ProjectLast Labs GC/LC MemoReportT Oct 11Process (on-Line)Analysis – Components(TAR)Open Lab Project NotebooksTH Oct13Process (on-Line)Analysis – Systems (TR)Open Lab Project/ LabCleanupLast Lab MemoReportT Oct 18The University of Utah seeks to provide equal access to its programs, services and activities for people with disabilities. If you will need accommodations in the class, reasonable prior notice needs to be given to the Center for Disability Services, 162 Olpin Union Building, 581-5020 (V/TDD). CDS will work with you and the instructor to make arrangements for