SC CHEM 321 - Design an Analysis: Choosing a Solvent (5 pages)

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Design an Analysis: Choosing a Solvent



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Design an Analysis: Choosing a Solvent

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Pages:
5
School:
University Of South Carolina-Columbia
Course:
Chem 321 - Quantitative Analysis

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Cameron Kahn Muditha Dias Experiment 6 Post Lab 2 April 2014 Experiment 6 Design an Analysis Choosing a Solvent Data Standard sample Retention time Retention Linalool 54 1mg Compound time min Carvone 51 3mg Carvone 8 851 Eugenol 66 4mg Cinnamaldehyd Cinnamaldehyd 68 6mg e 9 061 eLinalool 7 668 Eugenol 9 716 Hexane 1 Hexane 2 Hexane 3 Hexane 4 Hexane 5 Peak 1 2 3 4 Peak 1 2 Peak 1 2 Peak 1 2 3 4 Peak 1 2 Retention time min 8 4 9 845 11 099 12 216 Retention time min 11 092 12 209 Retention time min 11 092 12 208 Retention time min 3 561 9 84 11 092 12 209 Retention time min 3 565 9 841 Area 33781665 94702316 129836621 146256402 Area 2877097 3170599 Area 2140479 2171796 Area 1681468 384823 1194871 925022 Area 1338244 258383 Diethyl 1 Diethyl 2 Diethyl 3 Diethyl 4 Diethyl 5 Ext Hexane 3 4 Peak 1 2 3 4 5 6 7 8 Peak 1 2 3 4 5 Peak 1 2 3 Peak 1 2 Peak 1 2 Peak 1 2 3 4 5 6 7 8 11 092 12 209 Retention time min 5 332 7 599 8 87 9 841 10 405 10 669 11 093 12 21 Retention time min 5 328 5 398 10 422 11 093 12 21 Retention time min 5 327 10 421 11 093 Retention time min 5 33 10 43 Retention time min 5 33 10 438 Retention time min 3 566 6 553 6 583 7 004 7 127 7 602 7 883 8 858 1028009 698198 Area 5516345 513446 331427 703932 2527230 184887 531566 252097 Area 2212687 2053424 1997559 519374 297530 Area 4205131 1718774 260326 Area 3915410 1598613 Area 3526238 1143825 Area 1490030 1691917 1987969 1876755 1763755 284326332 4099894 158796227 Ext Diethyl 9 Peak 1 2 3 4 5 6 7 Standards 9 081 Retention time min 6 58 7 004 7 141 7 594 7 887 8 853 10 419 2053379 Area 1659910 901954 742805 177660621 1924850 92799763 2672162 Hexane as solvent concentration Retention area x y linalool 0 006492 0 00541 0 004328 0 003246 0 002164 Carvone 0 006156 33781665 0 00513 0 004104 0 003078 0 002052 Eugenol 1 0 007968 94702316 2 0 00664 3 0 005312 4 0 003984 384823 5 0 002656 258383 Cinnamaldehyd 0 008232 e 0 00686 0 005488 0 004166 0 00274 Diethyl Ether as solvent concentration Retention area y x 0



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