CATALOG DESCRIPTIONSTUDENT LEARNING OUTCOMESGENERALPre-requisites and Co-requisiteA grade of “C-” or better in General Chemistry I and II with lab (CHEM 211/211L and 212R /212LR), or the equivalent courses, is required for enrollment in this course. There is also a co-requisite of CHEM 321 Lecture.Pre-lab lectures and announcementsRequired materialsGRADING/ASSESSMENTDuring the pre-lab lecture, the GTAs will tell you what you need to hand in for your report on that lab. You will turn in nine lab reports, each worth 20 points (an additional lab (lab number 7) is an extended lab report and is worth 30 points). You...Laboratory Performance and Technique:Part of the grade for each lab report will include a score for laboratory performance and technique. You are expected to be prepared for lab, maintain your drawer, space and wastes appropriately, wear safety goggles/glasses and proper attire at all t...POLICIESEnrollment and AttendanceYou must be enrolled in the section you are attending. If you are not enrolled by the end of the second week of classes (September 5th), you will be asked to leave the lab. Attendance is required and will be taken by GTAs at all laboratory classes. ...Safety and HonestyLaboratoryLab ReportsLAB NOTEBOOKSLAB REPORTSBefore lab ( Pre-labA copy of this statement will be provided for your signature before the first experimentChemistry 321L Fall Semester 2014 Organic Chemistry Lab I (Chemistry 321L, 1 credit) Syllabus Organic Lab Coordinator: Dr. Andrea Drew Gounev ([email protected]) Associate Teaching Professor Office: Flarsheim Hall 510D Office Hours W 11:00am-12:00pm, and by appointment Course Website: http://d.web.umkc.edu/drewa/Chem321L/index321L.html Meets Day Time Teaching Assistants (Office Hours on Blackboard)) Instructor in charge SCB 212 M 2:00 - 4:50 PM (V01) 40193 Gerald Corsiglia ([email protected]) Fei Wu ([email protected]) Dr. Drew Gounev SCB 212 T 8:00 - 10:50 AM (V03) 40195 Dayu Wang ([email protected]) Brian McEntee ([email protected]) Dr. Drew Gounev SCB 212 T 11:00AM - 1:50 PM (V09) 45095 Alok Nerurkar ([email protected]) Dattatray Sawant ([email protected]) Dr. Drew Gounev SCB 212 T 2:00 - 4:50 PM (V04) 40196 Lincoln Maina ([email protected]) Dattatray Sawant ([email protected]) Dr. Drew Gounev SCB 212 W 2:00 - 4:50 PM (V02) 40194 Fei Wu ([email protected]) Gerald Corsiglia ([email protected]) Dr. Drew Gounev SCB 212 R 8:00 - 10:50 AM (V06) 40198 Dayu Wang ([email protected]) Fei Wu ([email protected]) Dr. Drew Gounev SCB 212 R 2:00 - 4:50 PM (V05) 40197 Alok Nerurkar ([email protected]) Brian McEntee ([email protected]) Dr. Drew Gounev SCB 212 F 8:00 - 10:50 AM (V07) 40199 Dayu Wang ([email protected]) Dr. Drew Gounev SCB 212 F 2:00 - 4:50 PM (V08) 40200 Gerald Corsiglia ([email protected]) Brian McEntee ([email protected]) Dr. Drew Gounev CATALOG DESCRIPTION CHEM 321L introduces the student to basic techniques and procedures in isolation, purification, and characterization of organic compounds and simple reactions used in the organic chemistry laboratory. The student will also be trained in the proper way to write a scientific laboratory report. Prerequisite: CHEM 211/CHEM 211L and CHEM 212/CHEM 212L or their equivalents (each with a C-or better) Restrictions: corequisite CHEM 321 Offered: Each Term. 1Chemistry 321L Fall Semester 2014 STUDENT LEARNING OUTCOMES Upon completion of Chemistry 321L, students should be able to: • Apply knowledge obtained in Chemistry 321 lecture to problem solving and critical thinking in the laboratory. • Utilize mathematical knowledge gained from general chemistry to perform common calculations, including mass balance, limiting reagent, and percent yield. • Engage in safe laboratory practices by handling laboratory glassware, equipment, and chemical reagents appropriately, using general guidelines and basic knowledge about the common hazards associated with them in an organic chemistry laboratory. • Maintain an appropriate scientific notebook using notational and descriptive content containing MSDS information on relevant chemical reagents, experimental procedure followed, data collected, and observations made during the experimental process. • Assemble glassware and perform the following techniques as a part of synthetic procedures: aqueous workup, distillation, reflux, separation, isolation, and crystallization. • Predict the outcome of several common organic reaction types through a basic understanding of starting materials, functional groups, mechanism, and typical reaction conditions. • Characterize prepared substances by physical and spectroscopic means. • Develop the skill set necessary to continue on to Chemistry 322L. GENERAL Pre-requisites and Co-requisite A grade of “C-” or better in General Chemistry I and II with lab (CHEM 211/211L and 212R /212LR), or the equivalent courses, is required for enrollment in this course. There is also a co-requisite of CHEM 321 Lecture. Pre-lab lectures and announcements All classes will convene in room C212 in the Spencer Chemistry Building before entering the lab for class announcements, pre-lab lectures, and submission of lab reports. Attendance will be taken in pre-lab. Required materials • Mohring et al. Techniques in Organic Chemistry, 4th ed.; 2014, W.H. Freeman (ISBN-10: 1464134227 and ISBN-13: 9781464134227). 3rd Edition ok too! This may be purchased from the UMKC Bookstore. • A lab notebook capable of making carbon copies (100 pages is a good size). The copies are submitted to your GTA as you leave the lab each session and become part of your report; you retain the originals. This may be purchased from the UMKC Bookstore. • Padlock, safety glasses, any color felt-tip pen with permanent ink (Sharpie). • Non-graphing calculator (like the one you used in General Chemistry I and II). • Appropriate clothing (i.e., no shorts, open-toed shoes, etc.). 2Chemistry 321L Fall Semester 2014 GRADING/ASSESSMENT During the pre-lab lecture, the GTAs will tell you what you need to hand in for your report on that lab. You will turn in nine lab reports, each worth 20 points (an additional lab (lab number 7) is an extended lab report and is worth 30 points). Your lowest lab score (from the twenty point labs) will be dropped (if you have an “excused” lab, it will be your dropped lab), for a total of 190 points for your reports.